LABORATORY
ACCURACY
QUALITY CONTROL
PROFICIENCY TESTING PROGRAMS
PROCEDURES AND METHODS
ASSOCIATIONS
 
 
PROCEDURES AND METHODS 

When comparing results from one laboratory to the next it is important to determine the following:

Laboratory methods used by each laboratory for each analysis.
Units reported by each laboratory for each analysis.
Any conversion or calculation used by each laboratory.

If any of these variables are unknown, it will not be possible to complete a data comparison.

It is important to note that there is no perfect method for determining how much or little of an essential nutrient is available for plant uptake. Availability is determined by: soil moisture, temperature, soil pH, clay content, soil drainage, organic content, physical barriers, and many other factors. As any of these factors change, the availability will also change.

 
METHODS USED BY HARRIS LABORATORY: SOIL ANALYSIS, PLANT ANALYSIS, MEDIA TESTING

References used for Laboratory Methodologies.

Analytic procedures used in US EPA Report SW-846, Test Methods for Evaluating Solid Waste, 3rd Edition, November 1990, as revised.

Association of Official Analytical Chemists (AOAC) Official Methods of Analysis, 1990, 15th edition.

Methods of Soil Analysis, Parts I, II and III. Soil Science Society of America. 1996
North Central Regional (NCR) Publication No. 221 (Revised). Recommended Chemical Soil Test Procedures for the North Central Region Bulletin No. 499 (Revised) October 1988.

Standard Methods for the Examination of Water and Wastewater, 18th Edition, 1992.

The American Society for Testing and Materials (ASTM) Standard Test Methods, 1988.

Laboratory Methods Used by: Harris Laboratory
Analysis Units Method Description
SOIL ANALYSIS
Soil pH N/A 1:1 Soil/Water Slurry
Soluble Salt mmhos/cm 1:1 Soil/Water Slurry
Buffer pH N/A SMP Buffer Solution
Cations
Ca-Mg-K-Na
ppm Ammonium Acetate Extraction
Phosphorus
    If pH<7.2
    If pH>7.1
ppm
ppm
Bray I Extraction
Olson Extraction

Traces
Zn-Mn-Fe-Cu

ppm DTPA Extraction
Sulfur ppm Monocalcium Phosphate
(ICP Determination)
Boron ppm Hot Water Extraction
(ICP Determination)
Nitrate-N ppm Cadmium Reduction
Particle Size Analysis
(Sand-Slid-Clay)
% Hydrometer Measurement
Salinity Evaluation mmhos/cm Saturated Paste Extraction

PLANT ANALYSIS
Nitrate-Nitrogen ppm 2% Acetic Acid digestion
Phosphate-Phosphorus ppm 2% Acetic Acid digestion
Extractable Potassium % 2% Acetic Acid digestion
Total Nitrogrn % Kjedahl Digestion
Total Phosphorus % Nitric Acid/Hydrogen Peroxide Digestion

GREENHOUSE MEDIA TESTING
Media pH N/A Saturated Media Extract (SMS)
Electrical Conductivity mmhos/cm "
Phosphorus ppm "
Potassium " "
Calcium " "
Magnesium " "
Sodium " "
Zinc " "
Manganese " "
Copper " "
Iron " "
Boron " "
Aluminum " "
Nitrate-N " "
Ammonium-N " "
Extractable Zinc
  Manganese
  Copper
  Iron

ppm
"
"
"

DTPA Extraction
"
"
"
Organic Matter & % Loss on Ignition
Organic Carbon    
Total Nitrogen % Kjedahl Digestion
Soluble P2O5 % Citric Acid Digestion
Soluble K2O % Ammonium Oxalate